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Pią 23:15, 18 Mar 2011 |
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Dołączył: 17 Gru 2010
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Temat postu: Achyranthes Isolation and identification of _2213 |
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Achyranthes Isolation and identification of
. 9839.639,539.56 a Me52.1948.048.048.06 a Bu1037.036.936.9165.0ll23.823.723.723O. 812122.6122.9122.6319.21314-4.914-4.114-4.1413.71442.242.142.11528.428.328.213-D-Glcl623.823.423.4 】 ,, lo6. 1105.9l05.91746.746.246.2277.477.677.61842.041.841.73 878.077.92134.234.034.0662.862.862.72233.333.133.12328.228.128.128 a B-D-Glc2416.816.716.7195.895.72515.515.515. 5274.274.12617.417.517.5379.379.32726.226.I26.1471.271.12818O.1176.4176.4579.078.92933.332.632.5662.362.23O23.823.823. 8 The results showed that acid hydrolysis : molecules containing glucose and glucuronic acid . HMBC spectrum showed n-butyl C-1 Glucuronic acid connected on 6 . Compound 6 was therefore inferred V Panax japonicus butyl glycosides (chikusetsus India 0ninVbutylester). H. NMR (300MHz,[link widoczny dla zalogowanych], PY-d5): 60.84,[link widoczny dla zalogowanych],0.87,0.90,1.07,1.07,1.24,1.24 (each, 3H, s), 4.94 (1H, d, J = 6.9Hz,[link widoczny dla zalogowanych], GlcAH.1),[link widoczny dla zalogowanych], 65.36 (1H, d.J = 7.6Hz, GlcH.1 ), 65.41 (1H, br.s, H-12); Thanks MS from the Institute of Chinese Medicine , China Pharmaceutical University teacher of measurement Xu Ran , C H NMR spectrum by the China Pharmaceutical University,[link widoczny dla zalogowanych], a teacher of Analysis and Testing Center Chendong Jun measure , I would like to thank caused .
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